New NIST-traceable standards for calibration and validation of DSC
Identifieur interne : 008769 ( Main/Repository ); précédent : 008768; suivant : 008770New NIST-traceable standards for calibration and validation of DSC
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Abstract
Several reference materials and associated reference values have been recommended for the purposes of calibration and/or validation of differential scanning calorimetry (DSC). However, issues of available sample purity, reference-property value accuracy, and potential undesired reactions between reference materials and the materials used for sample pans have not been considered sufficiently in some of the recommendations of property values for the materials. These limitations attenuate greatly the usefulness of many of these reference material recommendations. Indeed, the state of uncertainty regarding true reference property values can be shown to be a limiting factor in the uncertainty of measurements made with DSC. NIST has certified the temperatures and enthalpies of fusion of two new Standard Reference Materials, SRMs 2234 and 2235, in order to help alleviate some of the difficulty.
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">New NIST-traceable standards for calibration and validation of DSC</title><author><name sortKey="Archer, D G" uniqKey="Archer D">D. G. Archer</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Physical and Chemical Properties Division, National Institute of Standards and Technology, 100 Bureau Drive, MS 8380</s1><s2>Gaithersburg, MD 20899-8380</s2><s3>USA</s3><sZ>1 aut.</sZ></inist:fA14><country>États-Unis</country><placeName><region type="state">État du Mississippi</region></placeName></affiliation></author></titleStmt><publicationStmt><idno type="inist">07-0022552</idno><date when="2006">2006</date><idno type="stanalyst">PASCAL 07-0022552 INIST</idno><idno type="RBID">Pascal:07-0022552</idno><idno type="wicri:Area/Main/Corpus">008459</idno><idno type="wicri:Area/Main/Repository">008769</idno></publicationStmt><seriesStmt><idno type="ISSN">1388-6150</idno><title level="j" type="abbreviated">J. therm. anal. calorim.</title><title level="j" type="main">Journal of thermal analysis and calorimetry</title></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Bismuth</term><term>Calibration</term><term>Certification</term><term>Differential scanning calorimetry</term><term>Gallium</term><term>Indium</term><term>Reference material</term><term>Standard</term><term>Thermal analysis</term><term>Tin</term><term>Traceability</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Etalonnage</term><term>Calorimétrie différentielle balayage</term><term>Bismuth</term><term>Gallium</term><term>Indium</term><term>Etalon</term><term>Matériau référence</term><term>Etain</term><term>Certification</term><term>Traçabilité</term><term>Analyse thermique</term></keywords><keywords scheme="Wicri" type="concept" xml:lang="fr"><term>Bismuth</term><term>Traçabilité</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Several reference materials and associated reference values have been recommended for the purposes of calibration and/or validation of differential scanning calorimetry (DSC). However, issues of available sample purity, reference-property value accuracy, and potential undesired reactions between reference materials and the materials used for sample pans have not been considered sufficiently in some of the recommendations of property values for the materials. These limitations attenuate greatly the usefulness of many of these reference material recommendations. Indeed, the state of uncertainty regarding true reference property values can be shown to be a limiting factor in the uncertainty of measurements made with DSC. NIST has certified the temperatures and enthalpies of fusion of two new Standard Reference Materials, SRMs 2234 and 2235, in order to help alleviate some of the difficulty.</div></front></TEI><inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>1388-6150</s0></fA01><fA03 i2="1"><s0>J. therm. anal. calorim.</s0></fA03><fA05><s2>85</s2></fA05><fA06><s2>1</s2></fA06><fA08 i1="01" i2="1" l="ENG"><s1>New NIST-traceable standards for calibration and validation of DSC</s1></fA08><fA09 i1="01" i2="1" l="ENG"><s1>33rd North American Thermal Analysis Society Conference: NATAS 2005, September 19-21, 2005, Universal City, California</s1></fA09><fA11 i1="01" i2="1"><s1>ARCHER (D. 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Indeed, the state of uncertainty regarding true reference property values can be shown to be a limiting factor in the uncertainty of measurements made with DSC. 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